Metrohm 861 Advanced Compact IC - Manual (Page 5)

Table of contents
861 Advanced Compact IC / Instructions for Use 8.861.1033
I
Table of contents
1 Introduction ................................................................ 1
1.1 Instrument description ................................................................................1
1.2 Parts and controls .......................................................................................3
1.2.1 Front.................................................................................................................... 3
1.2.2 Rear panel .......................................................................................................... 4
1.2.3 Interior 2.861.0010.............................................................................................. 5
1.2.4 Interior 2.861.0020.............................................................................................. 7
1.2.5 Interior 2.861.0040.............................................................................................. 9
1.3 Information on the Instructions for Use ...................................... .............11
1.3.1 Organization ..................................................................................................... 11
1.3.2 Notation and pictograms.................................................................................. 12
1.4 Safety notes ...............................................................................................13
1.4.1 Electrical safety................................................................................................. 13
1.4.2 General precautionary rules ............................................................................. 13
2 Installation ............................................................... 14
2.1 Overview ....................................................................................................14
2.1.1 Flow chart ......................................................................................................... 14
2.1.2 Connections in the 861 Advanced Compact IC .............................................. 14
2.2 Setting up the instrument..........................................................................16
2.2.1 Packaging......................................................................................................... 16
2.2.2 Check................................................................................................................ 16
2.2.3 Location ............................................................................................................ 16
2.3 Attaching the accessories.........................................................................17
2.3.1 Connection of detector block........................................................................... 17
2.3.2 Connection of syringe and aspirating tubing................................................... 18
2.3.3 Connection of the drain tube for the inner compartment ................................ 18
2.3.4 Connection of the drain tube for bottle rack .................................................... 18
2.3.5 Connection of PEEK capillaries........................................................................ 18
2.3.6 Filter unit PEEK ................................................................................................. 19
2.4 Mains connection ......................................................................................21
2.4.1 Setting the mains voltage................................................................................. 21
2.4.2 Fuses ................................................................................................................ 22
2.4.3 Mains cable and mains connection ................................................................. 22
2.4.4 On/off switching of the instrument ................................................................... 22
2.5 Connection to PC ......................................................................................23
2.5.1 Connecting cable ............................................................................................. 23
2.5.2 Software installation.......................................................................................... 23
2.5.3 First Login ......................................................................................................... 24
2.5.4 Create a system ............................................................................................... 24
2.6 High-pressure pump .................................................................................25
2.6.1 Removing the transport security screws.......................................................... 25
2.6.2 Installing the pulsation dampener.................................................................... 25
2.6.3 Connecting the eluent bottle ............................................................................ 26
2.6.4 Deaerating the pump and rinsing the pulsation dampener............................. 28
2.7 Precolumns and separating columns ......................................................30
2.7.1 Precolumns....................................................................................................... 30
2.7.2 General information on separating columns ................................................... 31
2.7.3 Selecting the sample loop................................................................................ 31
2.7.4 Installation of the separating column without suppressor module «MSM II» .. 32
2.7.5 Installation of the separating column with suppressor module «MSM II» ....... 33