15 metrohm co2 suppressor (mcs), 1 general information on the mcs, 2 connecting mcs – Metrohm 882 Compact IC plus – Anion – MCS User Manual
Page 58: 15 metrohm co, Suppressor (mcs), General information on the mcs, Connecting mcs
3.15 Metrohm CO
2
Suppressor (MCS)
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882 Compact IC plus – Anion – MCS
4 Connecting the rinsing the solution outlet capillary
■
Guide the other end of the outlet capillary labeled with waste
rins. into a sufficiently large waste container and fasten it there.
5 Connecting the regeneration solution inlet capillary
■
With a short PEEK pressure screw (6.2744.070), fasten the end of
the inlet capillary labeled with regenerant to the pump tubing
connection of the pump tubing which carries the regeneration
solution.
6 Connecting the regeneration solution outlet capillary
■
Guide the other end of the outlet capillary labeled with waste
reg. into a sufficiently large waste container and fasten it there.
3.15
Metrohm CO
2
Suppressor (MCS)
3.15.1
General information on the MCS
The Metrohm CO
2
Suppressor (MCS) removes the CO
2
from the eluent
flow. This reduces the background conductivity, improves the detection
sensitivity and minimizes the injection and carbonate peaks.
CO
2
can reach the eluent flow through the sample itself or arise through
the suppression reaction in the MSM/. The CO
2
peak is effectively mini-
mized through connection of the MCS between the MSM and detector.
The principle of the MCS is based on the gas permeability of the fluoropol-
ymer membrane inside the degassing cell of the MCS. The eluent is guided
through a capillary with a fluoropolymer membrane inside the degassing
cell. A vacuum is generated in the degassing cell by the pump, at the
same time, the pump sucks CO
2
-free air – ambient air is aspired through a
CO
2
adsorption cartridge (26-4), which removes the CO
2
. The pressure
and concentration difference in the degassing cell in comparison to the
inside of the capillary now causes the CO
2
to diffuse out of the eluent
flow.
3.15.2
Connecting MCS
The MCS is connected between the MSM and detector.